The microfabrication lab (LMF) offers, to the academic and the industrial sector, a large cleanroom in order to perform research and prototyping work. Main fields are semiconductors, microfluidic and MEMS (Micro Electro Mechanical System). Most of the installations and equipment are able to handle small silicon, glass, III-V materials, or other substrate pieces to full 6 inch wafers. The laboratory is equipped to handle most of the common microfabrication steps: spin-coating, photolithography, e-beam lithography, metal and material deposition, chemical and plasma etch, metrology and inspection, bonding, wet chemistry and dicing.
We offer your the possibility of a VIRTUAL TOUR
Lithography is a central microfabrication step. Using photosensitive resist material, master patterns are transfered on the substrate surface. Many lithography and alignment steps over different material layers may be necessary to complete a device.
MA6 Mask Aligner
The MA6 is a contact mask aligner well adapted to the challenging and variable laboratory use, allying precision and flexibility. The aligner has double microscope field view and a backside CCD camera to allow fast and precise aligment for single and double side needs. It also allows the use of very small samples up to 6 inches full wafers.
Manufacturer : Karl Suss
Model : MA-6/BA-6
- Mask dimensions: ≤ 7″
- Sample size: 1cm2 to 6 in
- Contact modes: 5 available (hard vacuum to proximity)
- Lamp: 350W Hg
- Optics: UV 400 (436 – 405 – 365 – 335 – 313 nm lines)
- Exposure modes: Constant power or constant intensisty
- Alignment modes: Front to front/ back to front (optic)
Surface pretreatment oven
Substrate deshydration and HMDS activation are often key processes to get maximal adhesion of photoresist and surface cleanliness and stability for other processes.
The YES oven has several programmed recipies available, for vacuum or nitrogen environment dehydration and vapor deposition of HMDS precursor.
Manufacturer: Yield Engineering Systems
Model: YES-310TA
Number of programs available: 12
Silanisation material: HMDS
Photoresist coating
The photolithography room offers 2 spincoating stations.
BREWER SPINCOATER
Small part up to 200 mm wafers may be resist coated using this spincoater. The system include automatic dispense of edge bead removal and photoresist. All staedy state, acceleration and spinnning speeds are programmable.
The attached hotplate allows for high uniformity resist baking.
Manufacturer: Brewer Sciencce
Model: 200cbx
Development BENCH
The clean wet processing bench offers many accesories for manual developping steps and drying. High purity DI water is available.
Available photoresists PROCESSES
OIR 674-11 positive; 1 micron thick
AZ5214-EIR reversible resist ; used for lift off ; 1.5 microns thick
LOR5 non photosensitive; used for lift-off resist undercoat; 5 microns
KMPR 1005 negative resist, dedicated to DRIE processes, 5 microns
SU8 Resist (different thicknesses) negative resist, mainly used for microfluidic applications
AZ MiR 900
PMMA 950 A2 e-beam lithography resist
E-beam lithography permits to draw very high resolution features on substrates down to the nanometer range.
The technique uses a focalised electron beam as the drawing tool on resist precoated samples. Cad drawing tools are used to generate features.
The system also allows for very long path drawings, without stiching faults.
Spécifications techniques
Model : Raith e-line
Beam size: less than 2 nm at 20 kV
Beam energy: 100eV to 30 KeV
Beam current: 20 pA to 20 nA
Minimum linewidth: 20 nm (with PMMA950)
Accessories : FBMS (fixed beam moving stage)
Maximum sample size : 10cm
Maximale sample thickness : 2mm
Available resists
PMMA 495 A4
PMMA 950 A2
Copolymer PMMA EL 9
Ma-N 2401
The Picomaster 150 from Raith was installed in december 2024 in the cleanroom.
It is a ighresolution UV direct write tool avble to deliver high performance and process flexibility.
- Resolutions up to 300 nm
- sample size: form a few mm to 150 mm wafers.
- Write area up to 100 mm
- Optical Module with 375 nm wavelength
- Real-time laser controlled auto focus
- Direct drawing option on camera image
- 4095 grayscale levels
- Automatic switching between 4 write modes: 300, 500, 900 nm and 5 microns
- Area search with automatic marker recognition
- Top side alignement only
- up to 0.3 μm top side alignment accuracy
DEEP REACTIVE ION ETCHING (DRIE-ICP)
Deep Reactive Ion Etching – Inductively Coupled Plasma (DRIE-ICP) is a highly anisotropic process to create tridimensional features in a silicon wafer wafer or other materials. Its main strength is the high aspect ratio that can be reached, up to 30:1. Our DRIE-ICP features a high plasma density, a low pressure during the process, a high etching rate and a good etching uniformity. The DRIE is extensively used for MEMS manufacturing.
USES
- Deep etching of silicon
Technical specifications
Manufacturer : Oxford
Model : Plasmalab System 100 ICP 180
Process : | Cryo | Bosch |
Materials etched : | Si | Si |
Masks : | PR, SiO2, Cr | PR, SiO2, Cr |
Gases : | SF6, O2 | SF6, O2, C4F8 |
Etching rate : | > 2.5 µm/min | > 2 µm/min |
Selectivity : | > 75 :1 for positive resin, > 150 :1 for SiO2, ~infinite for Cr | |
Uniformity : | <±5% on 4 in. wafers | N/A |
Repeatability : | <±4% | <±5% |
Profile : | 90° ± 1° | 90° ± 1° |
Aspect Ratio : | Up to 30 :1 | Up to 30 :1 |
Reactive Ion Etching is mainly used to anisotropically etch complete or structured layers on microelectronic devices. The choice of gazes as well as their pressures and the plasma power allows for controlled etching of materials.
Technical specifications
Available gases: SF6, O2, N2, Ar, He, CF4, C4F8, CHF3
Materials: Si, SiO2, SiN, organics (photoresists, parylene …)
Sample size: few mm up to full 200 mm wafer
Plasma type: RF
Plasma power: 300W (max)
The SUSS SB6e allows bonding of materials together for micro electro-mechanical system applications. After positioning and alignment using the MA6 aligner, the substrates are moved to the SB6 and bonded using one of the various available processes such as: Anodic Bonding, Silicon Fusion Bonding (SFB), Adhesive Bonding (ADB), Thermal Compression Bonding (TCB).
SPECIFICATIONS
Manufactureer: Suss Microtech
Sample size (mm): 2,5*2,5 cm parts to full 150mm (6 in ) wafers
Aligment precision after bonding: 1 micron
Temperature (°C): room to 500 Celcius
Maximal applied strenght: de 300 N à 20 KN
Vacuum: 5.10-5 mBar
Available bonding techniques: fusion bonding, Glass frit bonding, direct bonding, polymer adhesive bonding, metal eutectique bonding, anodic bonding, diffusion bonding
Alignment method : Optical, on mask aligner (MA6).
Parylene coating is biocompatible, dielectric, and hermetic. The deposited layer is conformal on exposed surfaces and pinhole free. The evaporation method from a precursor allows deposition to controlled thickenesses from a few nanometer to many microns.
Parylene is a coating material suitable for many applications among these are printed circuits, electronic sensors, medical components and many other substrates.
System description
Manufacturier : Specialty Coating Systems
Modèle : PDS 2010
The saw allows the dicing of large wafers into individual chips. The precision of the tool maximize device yield.
Technical data
manufacturer: Advanced Dicing Technology
Model: ADT 7100 Provectus
minimal sample size: few mm parts
maximal sample size: 8 inches wafers
Maximal trench depth: 2,1 mm (realised)
Cutting speed: 0 to 600 mm/s
Spindle speed: 60 KRPM max, 1,2 KW
Blades: resin bond , hubbed nickel bond…etc
Blades diameter: 2 or 3 inches
Trench depth precision: 0.2 microns resolution with 2 micron precision.
Materials : Si, Glass, Pyrex, LiNBO3, SiO2, Ceramic, Si on Glass, Quartz, Aluminium, Ferrite…
SUPERCRITICAL DRYING (CPD)
Supercritical fluids are obtained by heating a gas above its critical temperature or by increasing the pressure above its critical level. Supercritical drying consists of adjusting the temperature and pressure to transform the solvent into a supercritical fluid and then in gas. The liquid present in the system is therefore completely removed. This method is often used in Micro-electro-mechanical systems (MEMS) because it prevents damage to the fine machinery of these devices during the transition of the solvent between liquid and gas.
USES
Remove the liquid phase from a system
Spécifications techniques
Manufacturer: Tousimis
Model: Autosamdri 815B
Samples: parcelles jusqu’à 100mm de diamètre (4po)
Drying fluid: CO2
Rapid Thermal Annealing is a process used in semiconductor manufacturing that consists of heating a wafer to modify its structural properties. Thermal treatments can activate dopants, relax internal stress, diffuse materials to the interface, cristallize an amorphous layer, etc.
USES
- Activate dopants
- Diffuse materials to the interface
- Relax stress
- Modify the microstructure of thin films (crystallization, densification, defect removal, etc)
Technical specifications
Substrates : Semiconductors, metals, inorganic dielectrics
Sample holder : 4 in. diameter
Steady-state temperature range : 400-1150 °C (max 1350 °C)
Steady-state cycling time : 1-300 s
UHP gases for purging : O2, N2, Ar
Temperature stability : +/- 7 °C
Temperature control :
- Above 800 °C : Optical pyrometer
- Below 800 °C : Thermocouple
Heating rate : 220 °C/s (10-300 °C/s)
Cooling rate : < 80 °C/s (depending on temperature)
Non-uniformity of the radiative flux : < + 0.25%
Manufacturer : AG Associates
Model : Heatpulse 410
The UV ozonizing oven releases a large quantity of ozone to clean surfaces of various materials that are processed by microfabrication. It is particularly effective to eliminate any organic remains.
USES
- Surface cleaning
- Hybrocarbide trace cleaning
- Effective cleaning of inorganic surfaces: Si, quartz, glass, AsGa, SiC, metals (Au, Ni, Fe,…)
Technical specifications
Manufacturer : UVOCS
Model : T10x10 OES
RODAGE/MEULAGE
La polisseuse MetPrep vous permet de polir vos échantillons dans le but de les amincir ou de les préparer pour faciliter par exemple une analyse de surface. Le choix du degré de rugosité est possible grâce au changement aisé du plateau abrasif. L’opération de l’appareil peut être faite en mode manuel ou automatique. Des solution de polissage (slurry) de différent calibres sont disponibles pour compléter le lissage.
Marque/Model: Allied High Tech MetPrep4
Taille d’échantillon: Gaufre 2’’, 4’’ ou 6’’
CMP
Le polissage mécano-chimique (en anglais, Chemical mechanical polishing ou CMP) est un processus de lissage des surfaces utilisant l’action combinée de forces mécaniques et chimiques. Il peut être considéré comme un hybride de la gravure chimique et du polissage par abrasion libre. L’usager a le contrôle sur la vitesse de rotation et la pression pour influer la qualité et la vitesse de polissage. Les solutions colloidales de polissage à base de silice sont (slurry) utilisées de façon standard mais d’autres formulations sont possibles.
Marque/Model: Strasbaugh 6EC
Taille d’échantillon: Gaufre 4’’ ou 6’’
The analytical probe station allows electrical measurements on any device before encapsulation. The probes are moved individually and allow a precision of one micron. The metallic cage around the station along with the low current cables guarantee RF measurements in an environment without light nor vibration. Sources and multimeters are at the disposal of the users.
TECHNICAL DESCRIPTION
Model : EB-6
Stage : 6″-6″
Stage travel : 2″-2″
Total microscope magnification : 20X à 100X
Resolution : one micron
Accessories : faraday and light shield, anti-vibration table, low current RF cables
The four point probe setup is an easy-to-use system to evaluate the surface resistivity of thin films or the volume resistivity of silicon substrates or other thin conducting materials. The measurement technique relies on two pairs of electrodes, one injecting the current and the other measuring the voltage. This method reduces the error due to the contact resistance between the electrodes and the material, an error typical of the traditional two terminal setups. In addition, GCM Lab setup can make measurements at various temperatures.
USES
Measure the surface resistivity of conducting thin films
Measure the volume resistivity of semiconductors
Determine the resistivity of conductors as a function of temperature
Technical specifications
Probe spacing : 1 mm
Probe radius : 100 µm
Probe material: : Tungsten carbide
Température de mesure : -30 °C to 150 °C
Models : Bridgetech probes, Keithley 220 current source, Agilent 34401A voltmeter, Temptronic TP3000 temperature controller
The GCM has access to several instruments that allow the deposition of metallic films ranging from a few atoms in thickness to several hundreds of manometers. These coatings are particularly useful for the electronic industry but can also be used as wear or corrosion barriers. The most commonly used elements include gold, chromium, titanium, aluminium and silver but most metals can be deposited.
Furthermore, the GCM is a partner of the Functional Coatings and Surface Engineering Laboratory (FCSEL) one of the largest advanced coating laboratories in North America.
SPUTTERING AND E-BEAM EVAPORATION SYSTEM
This system is specifically dedicated to thin film deposition (1 nm to a few microns thick). It features a vacuum chamber containing an electron-beam evaporation source (six crucibles) and three 4-inch diameter targets for magnetron sputtering. A hopper is used to put the samples in the deposition chamber. This apparatus can deposit high quality films with good control of the thickness and a high uniformity.
USES
- Thin film deposition of metals by evaporation
- Deposition of metals by sputtering
Technical specifications
General
Substrates : Semiconductors, metals, plastics
Sample holder : 4 in. diameter
Pumping time : 10 min
Base pressure : 1×10-7 torr
Sample holder temperature : up to 200 °C
Option for plasma pre-treatment of the sample surface
Evaporation
Number of crucibles : 6
Volume of crucibles : 15 cm3
Crucible – sample holder distance : 18 in
Thickness control : <1% error
Max non-uniformity on thickness : 1% for a 4 in. wafer
Deposition rate : 0.5 – 3 Angströms / s
Sputtering
Number of targets : 3 targets
Target dimensions : 4 in. diameter
Precision on thickness : 5%
Crucible – sample holder distance : 5 in
Gases available : Ar, N2, O2
Option for codeposition of alloys from two targets
Manufacturer : Homemade
Model : Homemade
The magnetron sputterer is used to deposit a large range of metals and dielectrics. The particles that impinge on the substrate surface have a higher energy (1 eV) than that obtained by evaporation (0.1 eV), which confers to the films a higher density and a better adhesion. Reactive sputtering is also available with this system, to deposit oxides or nitrides. A hopper provides quick charging of the samples in the deposition chamber.
USES
Thin film deposition of metals and dielectrics
Technical specifications
Substrates : Semiconductors, metals, plastics
Sample holder : 4 in diameter
Base pressure : 5×10-7 torr
Pumping time : 10 min
Target sample holder distance : 5 in
Gases available : Ar, N2, O2
Number of magnetrons : 3
Thickness precision : 5%
Deposition rate : 1 – 10 Angströms / s
Manufacturer : Homemade
Model : Homemade
The electron-beam evaporator is used to deposit metals and dielectrics. It can deposit up to 6 materials successively while the thickness is precisely controlled by a microbalance. It is also possible to replace the materials after each deposition.
Uses
Deposition of metals and dielectrics on small samples
Technical specifications
Substrates : Any except plastics and photoresins
Sample holder : 4 in. diameter
Base pressure : 1×10-6 torr
Pumping time : 1h
Crucible – sample holder distance : 10 in
Number of crucibles : 6
Volume of crucibles : 1 cm3
Deposition rate : 1 – 10 Angströms / s
Manufacturer : Edwards
In thermal evaporation, the material to deposit is put in a crucible that is heated by the Joule effect. The material evaporates and is then deposited on the substrate.
USES
- Deposition of aluminium and gold films
Technical specifications
Substrates : Semiconductors, metals, plastics
Crucible – sample holder distance : 5 in
Metals deposited: gold and aluminium